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Which specifications belong on a nitriding drawing?

Which specifications belong on a nitriding drawing?

Nitride layer specification:

  • Surface hardness in HV
  • Core hardness in HV
  • Layer thickness specifications
    (diffusion layer and compound layer)
  • Nitriding hardness depth

Depending on the application, process and material, not all specifications need to appear on the drawing. We are happy to advise you.

Other important information for the party performing the nitriding:

  • Material specification
  • Heat treatment state
  • Measurement point indication
  • Areas that must be heat-treated
  • Areas allowed to be heat-treated
  • Areas not allowed to be heat-treated

You can find information on the comparability of the hardness in HV with other processes for hardness testing in the following hardness comparison table.

Expert knowledge on the subject

Surface hardness::

The surface hardness is the hardness value measured directly on the surface of your component. This is a measure for the mechanical resistance with which the component opposes the mechanical intrusion of another body. Amongst other things, it is therefore a measure of resistance to abrasive wear.
During plasma nitriding, the surface hardness is determined using a Vickers hardness tester. Depending on the layer thickness and surface hardness, testing is performed with a variable load.

In addition to the required hardness value, the test process and the test force (in kilogram-force) is also specified on the drawing.
Example: Surface hardness 610 HV1
Here, 610 is the hardness value, HV is the Vickers hardness test process and 1 is the test force of 1 kilogram-force.

The table provides an indication about which load is suitable for the test.

Core hardness:

The core hardness refers to the hardness which is measured in the core of the component. The core hardness is often measured in the metallographic cut.
For flawless nitriding, the core hardness should not change substantially compared to the core hardness of the untreated component.

The core hardness is also measured based on the Vickers process. The drawing specification is made by specifying a hardness value and the test load. A minimum and a maximum hardness value can be specified within which the core hardness should be.

The specification of a maximum hardness is useful if excessively deep nitriding is to be ruled out. The specification of a minimum hardness is primarily important for hardened materials if tempering is to be ruled out through the nitriding process.

Layer thickness specifications:

For materials which form a compound layer, it can be useful to specify the thickness of the compound layer. The same applies to high-alloy materials which only form a diffusion layer. Depending on the application, a minimum layer thickness and, if necessary, also a maximum layer thickness are specified. The specification is in µm.

Example 1: Compound layer thickness (CLT): 5–15 µm
Example 2: Diffusion layer thickness (DS): 5–25 µm

Nitriding hardness depth:

The nitriding hardness depth (DIN 50190T3), abbreviated to NHD, is defined as the vertical distance from the surface of a nitrided workpiece to the point at which the hardness corresponds to a defined hardness value. This hardness value is referred to as the hardness limit. A common definition for the hardness limit is the following:

Hardness limit = core hardness + 50 HV
Rounding to 10 HV occurs here. Test forces deviating from HV 0.5 are possible in the range HV 0.3 to HV 2.

Which specifications belong on a nitriding drawing?

Recommended maximum test loads to measure surface hardness, depending on NHD and expected Vickers surface hardness

Minimum
nitriding
depth (mm)
Expected minimum surface hardness (HV)
200-300 300-400 400-500 500-600 600-700 700-800 über 800
0,05 - - - HV 0,5 HV 0,5 HV 0,5 HV 0,5
0,07 - HV 0,5 HV 0,5 HV 0,5 HV 0,5 HV 1 HV 1
0,08 HV 0,5 HV 0,5 HV 0,5 HV 0,5 HV 1 HV 1 HV 1
0,09 HV 0,5 HV 0,5 HV 0,5 HV 1 HV 1 HV 1 HV 1
1 HV 0,5 HV 1 HV 1 HV 1 HV 1 HV 1 HV 3
0,15 HV 1 HV 1 HV 3 HV 3 HV 3 HV 3 HV 5
0,2 HV 1 HV 3 HV 5 HV5 HV 5 HV 5 HV 5
0,25 HV 3 HV 5 HV 5 HV 5 HV 10 HV 10 HV 10
0,3 HV 3 HV 5 HV10 HV 10 HV 10 HV 10 HV 10
0,4 HV 5 HV 10 HV 10 HV 10 HV 10 HV 30 HV 30
0,45 HV 5 HV 10 HV 10 HV 10 HV 30 HV 30 HV 30
0,5 HV 10 HV 10 HV 10 HV 30 HV 30 HV 30 HV 30
0,55 HV 10 HV 10 HV 30 HV 30 HV 30 HV 50 HV 50
0,6 HV 10 HV 10 HV 30 HV 30 HV 50 HV 50 HV 50
0,65 HV 10 HV 30 HV 30 HV 50 HV 50 HV 50 HV 50
0,7 HV 10 HV 30 HV 50 HV 50 HV 50 HV 50 HV 50
0,75 HV 30 HV 30 HV 50 HV 50 HV 50 HV 100 HV 100
The maximum permissible values ​​are listed. Of course, lower test loads may also be used, e.g. HV 10 instead of HV 30.